Electron energy loss spectroscopy of a TiAlN coating on stainless steel
15
Citation
15
Reference
10
Related Paper
Citation Trend
Keywords:
Energy-dispersive X-ray spectroscopy
Energy-dispersive X-ray spectroscopy
Cite
Citations (15)
Energy-dispersive X-ray spectroscopy
Characterization
Electron spectroscopy
Cite
Citations (7)
Energy-dispersive X-ray spectroscopy
Electron spectroscopy
Cite
Citations (7)
Abstract In none of these loss spectroscopies is spatial resolution required, but they do require electron sources capable of variable primary energy down to very low energies, with good stability. The need in HREELS for careful screening of the whole analytical system of source and analyser from strong magnetic fields has already been emphasized, as has the practice of minimizing currents of unwanted secondary electrons by coating internal surfaces with a low secondary emitter such as carbon.
Energy-dispersive X-ray spectroscopy
Electron spectroscopy
Secondary electrons
Cite
Citations (0)
Energy-dispersive X-ray spectroscopy
Reflection
Electron spectroscopy
Cite
Citations (0)
Mouse peritoneal free cells were observed in thick sections, 1 to 1.5 μm in thickness, by the transmission electron microscope operating at an accelerating voltage of 75 or 125 kV. Electron microscopy in thick sections provided valuable images for classifying the peritoneal cells and understanding their three-dimensional features.
Cite
Citations (3)
Energy-dispersive X-ray spectroscopy
Cite
Citations (16)
Energy-dispersive X-ray spectroscopy
Electron spectroscopy
Cite
Citations (1)
The use of electron energy loss spectroscopy (ELS) for elemental analysis of thin films holds considerable promise. This technique has definite advantages in comparison with energy dispersive X-ray spectroscopy (EDS) for two fundamental reasons. First, the detection sensitivity is independent of the fluorescence yield, since for each inner shell excitation an energy loss electron exists as opposed to only a finite probability that an excitation will result in a X-ray emitted. Second, the information carrying energy loss electrons are contained in a small solid angle about 0° scattering angle as opposed to the resulting X-rays which are emitted uniformly over 4Π steradians. This means that a large fraction of the energy loss electrons can be detected (up to ∼90%) compared to only a small fraction (∼1%) of the emitted X-rays with an EDS system.
Energy-dispersive X-ray spectroscopy
Electron scattering
Electron spectroscopy
Cite
Citations (1)
The microstructure of LiAlD4 with TiCl3·1/3(AlCl3) and VCl3 additives has been studied during different steps of the decomposition process using electron energy loss spectroscopy and energy-dispersive X-ray spectroscopy in a scanning transmission electron microscope. Energy filtered transmission electron microscopy was used to show elemental distributions in the samples. The spatial distribution of the additives and the main elements within the alanate particles was examined with a resolution of a few nanometers. The analysis of the electron energy loss spectra reveals the chemical state of Al, O, and the additives. Ti and V do not appear to mix chemically with Al to a significant degree. V was found in high concentration in just a few particles, while Ti is more uniformly distributed. All the samples showed evidence of oxidation despite procedures being adopted to avoid exposing the material to air. The additives are oxidized in all the samples, and Al2O3 forms a thin layer at the surface of the particles. This paper gives a comparison between samples at different stages of the decomposition process using different additives.
Energy-dispersive X-ray spectroscopy
Nanometre
Cite
Citations (20)