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    Abstract M r = 313.11, orthorhombic space group Pbca, a = 8.165(1), b = 9.491(2), c = 32.207(5) Å V = 2496(1) Å 3 , D X = 1.667 Mgm −3 , Z = 8, F(000) = 1248, λ(MoKα) = 0.71069 Å, μ = 32.7 mm −1 . The crystal structure was determined by direct methods and refined by least‐squares procedure to the discrepancy factor R = 0.065. Positions of hydrogen atoms were calculated. The structure determined by x‐ray analysis confirms the chemical results.
    Orthorhombic crystal system
    Crystal (programming language)
    Citations (0)
    Abstract The crystal and molecular structure of 1-(4-methoxyphenyl)-3-(phenyl)-2-propen-1-one derivative is determined by X-ray diffraction method. The compound, C16H14O2, crystallises in the orthorhombic space group Pbca with a=10.921(2) Å, b=30.583(1) Å, c=7.535(3) Å, V=2516.7(9) Å3, Z=4, D calc=1.242 Mg/m3, μ=0.327 mm−1, F 000=504, λ(MoKα)=0.71069 Å and the structure was refined to R=0.044.
    Orthorhombic crystal system
    Derivative (finance)
    Crystal (programming language)
    Chalcone
    Citations (1)
    A novel synthesis method of fibrillar trimolybdates with the use of Ag 2 Mo 3 O 10 ∙2H 2 O as a precursor has been used successfully to synthesize methylammonium trimolybdate, (CH 3 NH 3 ) 2 Mo 3 O 10 ∙H 2 O. The crystal structure of this compound was determined by X-ray powder diffraction method and refined by the Rietveld method. The compound is orthorhombic, space group P n m a (62), with a =11.241(3), b =7.585(1), and c =15.516(4) Å. The redetermined crystal structure of the precursor and the structure of the title compound are compared and discussed.
    Orthorhombic crystal system
    Rietveld Refinement
    Powder Diffraction
    Crystal (programming language)
    Citations (6)
    A crystal of 2,3-dimethyl-1-isopropylimidazolium bromide was prepared and its crystal structure determined at the orthorhombic space group Pnma with cell parameters a = 11.407(6), b = 7.157(4), c = 12.111(7)Å, Z = 4. Sandwiched structures were observed between the cations and the bromide anions. The π…Br and C-H…Br interactions contributed to stabilization of the crystal packing of the title compound.
    Orthorhombic crystal system
    Crystal (programming language)
    Citations (5)
    The compound C 36 H 26 N 4 O 4 , a derivative of Pigment Yellow 101, is one of the few organic pigments that show fluorescence in the solid state. Since single crystals could not be grown, the structure was determined from powder data. The X-ray powder pattern could be indexed with an orthorhombic unit cell. The space group remained ambiguous. The crystal structure was solved by lattice energy minimisation in different space groups using the program CRYSCA. Subsequently, the structure was refined by the Rietveld method using restraints. The compound crystallises in a herringbone pattern in Pbcn with a = 30.117(1) Å, b = 9.723(2) Å, c = 9.511(3) Å, Z = 4 with the molecule on an inversion centre. The insolubility and the solid-state fluorescence can be explained from the crystal structure.
    Orthorhombic crystal system
    Rietveld Refinement
    Powder Diffraction
    Crystal (programming language)
    Two novel compounds [Zn(dien)2]Te2(1) and [Ni(dien)2]Se3(2)(dien=diethylenetriamine) have been synthesized under the mild solvothermal conditions and characterized structurally.The crystal 1 belongs to orthorhombic space group Cmca with the lattice parameters a=9.212(2),b=10.854(3),c=15.723(4),Z=4.The crystal 2 belongs to orthorhombic space group Pna21 with the lattice parameters a=18.047(4),b=9.8236(19),c=9.0079(19),Z=4.The crystal structure of 1 consists of discrete dumbbell Te22- anions and distorted-octahedron [Zn(dien)3]2+ cations.Compound 2 consists of discrete 'V' shape Se32- anions and distorted-octahedron [Ni(dien)3]2+ cations.
    Orthorhombic crystal system
    Diethylenetriamine
    Dumbbell
    Lattice (music)
    Crystal (programming language)
    Citations (0)