Synthesis and Characterization of Colloidal Fluorescent Silver Nanoclusters
Sherry HuangChristian PfeifferJana HollmannSebastian FriedeJustin Jin-Ching ChenAndreas BeyerBenedikt HaasKerstin VolzW. HeimbrodtJosé María Montenegro MartosWalter H. ChangWolfgang J. Parak
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Abstract:
Ultrasmall water-soluble silver nanoclusters are synthesized, and their properties are investigated. The silver nanoclusters have high colloidal stability and show fluorescence in the red. This demonstrates that like gold nanoclusters also silver nanoclusters can be fluorescent.Keywords:
Nanoclusters
Characterization
Highly fluorescent Ag nanoclusters were prepared in aqueous solution via a rapid microwave-assisted green approach and used as a novel fluorescence probe for the determination of Cr(3+) ions with high sensitivity and excellent selectivity.
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Abstract The fluorescent gold nanoclusters (AuNCs) have been synthesized using aqueous reduction of chloroaric acid with mecapto undecanoic acid (MuA) as a thiol protecting agent. These AuNCs exhibited a strong absorption at 370 nm and a fluorescent emission in visible region. The emission spectrum can be tuned from 520 to 560 nm by controlling the NaOH concentrations during the reaction process. The gold nanoclusters exhibit a quantum yield of few percents and a fluorescence lifetime of ~2 ns. These properties of AuNCs provide greatly promising for biological applications.
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Бұл зерттеужұмысындaКaно моделітурaлы жәнеоғaн қaтыстытолықмәліметберілгенжәнеуниверситетстуденттерінебaғыттaлғaн қолдaнбaлы (кейстік)зерттеужүргізілген.АхметЯссaуи университетініңстуденттеріүшін Кaно моделіқолдaнылғaн, олaрдың жоғaры білімберусaпaсынa қоятынмaңыздытaлaптaры, яғнисaпaлық қaжеттіліктері,олaрдың мaңыздылығытурaлы жәнесaпaлық қaжеттіліктерінеқaтыстыөз университетінқaлaй бaғaлaйтындығытурaлы сұрaқтaр қойылғaн. Осы зерттеудіңмaқсaты АхметЯсaуи университетіндетуризмменеджментіжәнеқaржы бaкaлaвриaт бaғдaрлaмaлaрыныңсaпaсынa қaтыстыстуденттердіңқaжеттіліктерінaнықтaу, студенттердіңқaнaғaттaну, қaнaғaттaнбaу дәрежелерінбелгілеу,білімберусaпaсын aнықтaу мен жетілдіружолдaрын тaлдaу болыптaбылaды. Осы мaқсaтқaжетуүшін, ең aлдыменКaно сaуaлнaмaсы түзіліп,116 студенткеқолдaнылдыжәнебілімберугежәнеоның сaпaсынa қaтыстыстуденттердіңтaлaптaры мен қaжеттіліктерітоптықжұмыстaрaрқылыaнықтaлды. Екіншіден,бұл aнықтaлғaн тaлaптaр мен қaжеттіліктерКaно бaғaлaу кестесіменжіктелді.Осылaйшa, сaпa тaлaптaры төрт сaнaтқa бөлінді:болуытиіс, бір өлшемді,тaртымдыжәнебейтaрaп.Соңындa,қaнaғaттaну мен қaнaғaттaнбaудың мәндеріесептелдіжәнестуденттердіңқaнaғaттaну мен қaнaғaттaнбaу деңгейлерінжоғaрылaту мен төмендетудеосытaлaптaр мен қaжеттіліктердіңрөліaйқын aнықтaлды.Түйінсөздер:сaпa, сaпaлық қaжеттіліктер,білімберусaпaсы, Кaно моделі.
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Due to the polydispersity of nanocrystals and their unknown structures, in many cases it is difficult to conduct in-depth investigation on the sensing mechanism when nanocrystals are used as fluorescent probes; however, their smaller counterparts–structurally well-defined gold nanoclusters as sensors–have provided opportunities to do so. Herein, an example is provided by Wu et al. The potential of glutathione-capped Au25 nanocluster as silver-ion sensor is evaluated; more importantly, three factors are revealed to be responsible for the unique fluorescence enhancement of Au25(SG)18 illuminated in the image. This work is dedicated to the 30th anniversary of the Institute of Solid Physics, CAS.
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The nationally-recognized Susquehanna
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Metal nanoclusters consisting of a few to several tens of atoms have discrete energy states due to quantum size effects, which allows them to emit fluorescent. The fluorescent wavelength is dependent on the size of metal nanoclusters [1]. Much of studies on fluorescent metal nanoclusters have been focused on gold and silver. Recently we have succeeded in synthesizing platinum (Pt) nanoclusters which emit blue to yellow fluorescence [2-5]. Here we report on synthesis of fluorescent nanoclusters consisting of palladium (Pd) atoms.
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