Process for preparing active aluminium oxide
2003
The present invention relates to the preparation process of active gamma-Al2O3. The mixed water solution of materials including aluminum chloride, ammonia water, pore expander ammonium oxalate or ammonium citrate, etc. is heated and concentrated to produce aluminum hydroxide precipitate; the precipitate is dried and heated to obtain solid powder and to decompose its NH4Cl, which is recovered fromhot gas flow through cooling and crystallization; and the solid powder is roasted at 400-800 deg.c for 3-6 hr to convert into gamma-Al2O3. The present invention produces aluminum hydroxide through evaporation and concentration, rather than neutralization, and aluminium hydroxide is precipitated and separated in a stable and balanced solid-liquid state, and this is favorable to producing aluminiumhydroxide grains with homogeneous size.
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