DEOXYDATIVE SUBSTITUTION OF PYRIDINE 1-OXIDES. 18. TETRAHYDROPYRIDINES FROM 3-PICOLINE 1-OXIDE AND TERT-BUTYL AND 1-ADAMANTYL MERCAPTAN IN ACETIC ANHYDRIDE. STRUCTURAL ELUCIDATION BY LONG RANGE 2D J(C-H) RESOLVED NMR SPECTROSCOPY