Method for preparing nano composite material by supercritical fluid electroforming

The invention discloses a method for preparing nano composite material by supercritical fluid electroforming, which comprises the following steps of: (1) adding metal salt solution, nano granules and composite additive into a reactor of an electroforming device, stirring uniformly, introducing carbon dioxide gas, and stirring at the temperature of between 35 and 50 DEG C under the pressure of 8 to 20MPa to generate supercritical fluid electroforming solution containing the nano granules; (2) setting pulse interval at 1 to 5 microseconds, setting the pulse width at 10 to 30 microseconds, setting the current density at 1 to 3A/dm , switching on a direct-current power supply, and making the metal ions and the nano granules in the metal salt solution deposited on a cathode template togetherto obtain a nano composite electroforming layer; and (3) after the deposition is completed, obtaining the nano composite material by corresponding treatment. The method can electroform the nano composite material electroforming layer with uniform nano granule dispersion, flat surface, compact tissue, fine crystal grain and excellent performance.