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4-(2′,4′-二氟苯基)苯乙酮的合成及表征
4-(2′,4′-二氟苯基)苯乙酮的合成及表征
2008
Mengping Guo
Lin Yuan
Huirui Guo
zhangqiaochu
dengjihua
采用无配体Pd(Ⅱ)催化2,4-二氟苯硼酸与对溴苯乙酮的Suzuki偶联反应,35℃下,反应20min一步合成了标题化合物,偶联产率达98.7%,产物经IR、^1HNMR及晶体结构表征。
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