Determination of common anions in oxalate by ion chromatography coupled with UV photolysis pretreatment

Abstract A new and simple method was developed to determine anions in oxalate of analytical reagent grade. After UV photolysis with optimal 1% H 2 O 2 in 10,000 mg/L oxalate in the fabricated photoreactor, sample was directly injected into IC system. Satisfactory linearity, detections limits, good repeatability and spiked recovery were obtained. The method was successfully applied to determine anions in two commercial oxalate samples.