Process for preparing benorilate amyl alcohol

2015 
The invention belongs to the technical field of fine chemicals and relates to benorilate amyl alcohol, particularly a process for preparing benorilate amyl alcohol. According to the technical scheme of the invention, phenyl dihydro pyran is synthesized firstly, and then is hydrogenated preliminarily. The reaction liquid of phenyl dihydro pyran is filtered, and the filtered clear liquid is hydrogenated. After that, the filtered clear liquid is filtered and washed, and benorilate amyl alcohol can be obtained through decompressing and rectifying the obtained crude product. According to the invention, benorilate amyl alcohol is prepared by means of a Raney-Ni catalyst and a Pd/C catalyst successively through the secondary hydrogenation process, so that the hydrogenation yield is high. Meanwhile, enorilate amyl alcohol, as a final product, is large in yield. Therefore, the industrialization of the above process is high in production and promotion value.
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