Facile Green Synthesis of BCN Nanosheets as High‐Performance Electrode Material for Electrochemical Energy Storage

Two-dimensional hexagonal boron carbon nitride (BCN) nanosheets (NSs) were synthesized by new approach in which a mixture of glucose and an adduct of boric acid (H3BO3) and urea (NH2CONH2) is heated at 900 °C. The method is green, scalable and gives a high yield of BCN NSs with average size of about 1 μm and thickness of about 13 nm. Structural characterization of the as-synthesized material was carried out by several techniques, and its energy-storage properties were evaluated electrochemically. The material showed excellent capacitive behaviour with a specific capacitance as high as 244 F g−1 at a current density of 1 A g−1. The material retains up to 96 % of its initial capacity after 3000 cycles at a current density of 5 A g−1.