Conjugate Addition–Cyclization of a Cyanocuprate: 2‐Carbomethoxy‐3‐Vinylcyclopentanone
2003
Conjugate addition–cyclization of a cyanocuprate: 2-carbomethoxy-3-vinylcyclopentanone
intermediate: dimethyl (E)-2-hexenedioate
product: 2-carbomethoxy-3-vinylcyclopentanone
byproduct: Tetramethyltin
Keywords:
addition, to CC;
annulation, carbocyclic-[5];
cyclization, condensation;
metal-catalyzed reactions, palladium;
assay methods, of diastereomeric purity by nmr analysis;
lithium divinylcyanocuprate;
copper cyanide, poison;
copper cyanide, disposal;
methyllithium, ethereal solution of;
organotin compounds, disposal;
organotin compounds, poison;
tin alkyls, disposal;
tin alkyls, poison
Keywords:
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