Synthesis and spectroscopic characterization of palladium nanoparticles by using broth of edible mushroom extract

2011 
Reliable and eco-friendly process for the synthesis of metallic nanoparticles is an important step in the field of Nanoscience and Technology. In the present study we fabricate the palladium nanoparticles by using mushroom extract as a reducing and capping agent. It was observed that the synthesis procedure was quite simple and in a single step benign palladium nanoparticles were formed. UV-visible spectrum of the aqueous medium containing palladium ions demonstrated a peak corresponding to the plasmon absorbance of palladium nanoparticles. X-Ray diffraction (XRD) spectrum reveals the crystalline structure of palladium nanoparticles. The morphology of the biomolecules-stabilized palladium nanoparticles were determined by the atomic force microscopy (AFM) image. Energy dispersive X-ray analysis (EDS) evidences the presence of palladium nanoparticles in the aquatic solution of mushroom extract. FTIR analysis of the nanoparticles likewise indicated the possible presence of functional groups in biomolecules, which may be acting as capping agents around the nanoparticles.
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