Extension of gravity center method for diameter calibration of polystyrene standard particles with a metrological AFM
2012
In the particle diameter calibration using metrological AFM, the distance between center points of neighboring two
particles is referred to as "lateral diameter" when a single-layer close-packed structure of particles is successfully
formed. The distance between an apex of a particle and a substrate is referred to as "vertical diameter." In the previous
studies, lateral diameter was calculated by manually selecting and extracting a line profile from metrological AFM data
and directly applying a method to calculate a pitch of one-dimensional grating. As the manual line profile extraction
depends on who does it, however, there is a possibility that calculated lateral diameter is varied from person to person.
We developed a technology to calibrate diameter of polystyrene latex (PSL) particles by using our metrological AFM. In
this study, the gravity center method is extended to three dimensions to calculate position of and the center of gravity in
each particle. Lateral diameter, which was defined as distance between gravity centers of neighboring two particles, is
calibrated and uncertainty in the lateral diameter calibration is evaluated. Deformation of particles was also estimated by
using Young's modulus of thin film PSL and bulk PSL.
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