[CoL2]NO3的合成、晶体结构和红外光谱
2005
将水杨醛与N-2-羟乙基乙二胺按1:1物质的量混合,缩聚得到配体L,再分批加入等摩尔的Co(NO3)2·6H2O,制备出硝酸二(水杨醛N-2-羟乙基乙二胺缩席夫碱)合钴(Ⅲ),该配合物分子式[CoL2]NO3,属正交晶系,空间群为Fdd2,α=1.857 6(8)nm,b=5.696(2)nm,c=0.987 4(4)nm,V=10.448(8)nm3,α=β=γ=90.00°,Z=16.
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