Consolidation of W–Ta composites: hot isostatic pressing and spark and pulse plasma sintering

2015 
Abstract Composites consisting of tantalum fiber/powder dispersed in a nanostructured W matrix have been consolidated by spark and pulse plasma sintering as well as by hot isostatic pressing. The microstructural observations revealed that the tungstentantalum fiber composites consolidated by hot isostatic pressing and pulse plasma sintering presented a continuous layer of Ta 2 O 5 phase at the W/Ta interfaces, while the samples consolidated by spark plasma sintering evidenced a Ta + Ta 2 O 5 eutectic mixture due to the higher temperature of this consolidation process. Similar results have been obtained for the tungstentantalum powder composites. A (W, Ta) solid solution was detected around the prior nanostructured W particles in tungstentantalum powder composites consolidated by spark and pulse plasma sintering. Higher densifications were obtained for composites consolidated by hot isostatic pressing and pulse plasma sintering.
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