Evaluation of spectrographic standards for the carrier-distillation analysis of PuO/sub 2/

Three plutonium metals whose impurity contents have been accurately determined are used to evaluate spectrographic standards. Best results are obtained when (1) highly impure samples are diluted, (2) the internal standard, cobalt, is used, (3) a linear curve is fitted to the standard data that bracket the impurity concentration, and (4) plutonium standards containing 22 impurities are used.