Generation and Reactions of Alkenyllithium Reagents: 2‐Butylbornene
2003
Generation and Reactions of Alkenyllithium Reagents: 2-Butylbornene
reactant: 30.4 g (0.20 mol) of d-camphor
product: 2-Butylbornene
intermediate: 40.0 g (0.092 mol) of d-camphor 2,4,6-triisopropylbenzenesulfonylhydrazone
byproduct: bornylene
Keywords:
addition, to CO;
alkenylation, C-alkenylation;
alkylation, C-alkylation;
grignard and related reactions;
metalation reactions, lithium;
assay methods, for sec-butyllithium, with diphenylacetic acid or by double titration with benzoic acid and allyl chloride;
butyl bromide;
2-lithiobornene;
tetramethylethylenediamine
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