The novel continues biodiesel using ultrasound clamp tubular reactor
2014
Jatropha curcas oil (JCO), is used as the feedstock in this research work. The
work starts with design a new continuous process for biodiesel using ultrasound
clamp on tabular reactor for producing pure biodiesel from jatropha curcas oil
(JCO). Form this design, we fabricate the rig and test the application of
sonochemistry technique in biodiesel production through optimal and low cost
production technique for enhancing their capabilities and effective process.
Before run process of biodiesel the analysis of physical and chemical properties
of the feedstock and the associated product to obtain the major fatty acid
compositions of triglycerides applicable in the jatropha curcas oil. Based on
testing the free fatty acid of jatropha curcas oil is above 10.1 %. So for reduce
free fatty acid we need do esterification process using l%w/w of acid catalyst
and molar ratio methanol to oil is IS: 1 . After esterification, the free fatty acid of
the feedstock was testing and the result is 0.402%. It is important because is too
high free fatty acid it cause smaller the conversion efficiency. The next stage is
transesterification conducted with 6: 1, 9; 1 and 12: 1 molar ratio methanol to
jatropha for reaction times of 3, 5 and 7 minutes for 1% catalyst sodium
hydroxide (NaOH) at a temperature of 65OC with frequency arrange 17Hz to
22kHz and ultrasonic power output 240watt. The standard physical properties
test to determine the biodiesel qualities are flash point, water content, acid value,
density and dynamic viscosity. From test bed for continuous reactor using tubular
reactor the maximum producing biodiesel is 89 % was obtained with molar ratio
methanol to oil 6: 1 at 7 minutes reaction time.
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