Me3N-Promoted Synthesis of 2,3,4,4a-Tetrahydroxanthen-1-one: Preparation of Thiosemicarbazone Derivatives, Their Solid State Self-Assembly and Antimicrobial Properties.

Aminah Hameed,Zahid Shafiq,Muhammad Yaqub,Mazhar Hussain,Muhammad Ajaz Hussain,Muhammad Afzal,Muhammad Nawaz Tahir,Muhammad Moazzam Naseer

Me3N-Promoted Synthesis of 2,3,4,4a-Tetrahydroxanthen-1-one: Preparation of Thiosemicarbazone Derivatives, Their Solid State Self-Assembly and Antimicrobial Properties.

2016

Aminah Hameed
Zahid Shafiq
Muhammad Yaqub
Mazhar Hussain
Muhammad Ajaz Hussain
Muhammad Afzal
Muhammad Nawaz Tahir
Muhammad Moazzam Naseer

The title compound (III) is synthesized in high yield by Me3N-promoted domino Baylis—Hillman/oxa-Michael reaction sequence and smoothly converted into xanthene-based thiosemicarbazones (V).

Keywords:

Domino
Self-assembly
Antimicrobial
Semicarbazone
Xanthene
Solid-state
Chemistry
Organic chemistry
reaction sequence

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