Solvent Participation in a One‐Pot Glycosylation Strategy (SPOG)

Solvent participation in a one-pot glycosylation strategy (SPOG) was developed on the basis of the low concentration β - selective glycosylation method. This strategy enables the production of a β-glycosidic bond in a one-pot oligosaccharide synthesis without or with minimal use of any C-2 participating function.