Method for production of aromatic polyimide nanofiber based material
2015
FIELD: chemistry. SUBSTANCE: method is described for production of a polyimide nanofiber based material including electrospinning of polyamide acid solution in the solvent in which the solution containing not more than 12 wt % of polyamide acid in aprotonic solvent is used to obtain the film by the method of electrospinning through split draw die to the support; the film is removed from the support and dissolved, in the quantity ensuring polyamide acid content in the solution of 12-20 wt %, in the mixture aptoronic solvent : benzoid solvent with benzoid solvent content being 20-70 vol.%; the solution is supplied at room temperature through electrode- draw die to electric field with voltage of 15-35 kV; the material deposited on the anode is subjected to thermal treatment at a temperature of 370-420°C for 60 min; the target product consists of aromatic polyimide nanofibers with diameter of 50-700 nm and has decomposition temperature higher than 500°C in the inert medium in mixture. EFFECT: production of aromatic polyimide nanofiber based material using the method of electrospinning of polyamide acid at room temperature. 6 dwg, 5 ex
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