Novel preparative method for synthesis of isoindolo[2,1-b]benz-2-azepine-8-carboxylic acids
2003
Based on readily accessible homoallyl amines, we previously developed preparative methods for synthesis of substituted and spiro-annelated tetrahydroquinolines [1], 3-aza-11-oxatricyclo[6.2.1.01,6]undec-9enes (6,8a-epoxy isoquinolines) [2], γ-piperidoles [3], benz-2-azepines [4], isoindolo[2,1-a]quinoline-10carboxylic acids [5]. In continuing our work on studying the synthetic possibilities for furyl-substituted homoallyl amines, we carried out an original two-step synthesis for isoindolo[2,1-b]benz-2-azepine 3.
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