Trisammonium Geranyl Diphosphate

Trisammonium geranyl diphosphate reactant: 1.54 g (10 mmol) of geraniol intermediate: 0.83 g (4.8 mmol) of geranyl chloride product: trisammonium geranyl diphosphate Keywords: phosphonation; replacement reactions, halogen by diphosphate; replacement reactions, hydroxy by halogen; acetonitrile; buffer solutions, ammonium bicarbonate in aqueous isopropyl alcohol; buffer solutions, ammonium bicarbonate in aqueous isopropyl alcohol and acetonitrile; cation exchange resin, dowex ag 50w-xb, ammonium form; cellulose chromatography, preparation of column; N-chlorosuccinimide; dichloromethane (methylene chloride); tris(tetrabutylammonium) hydrogen pyrophosphate trihydrate, preparation from disodium dihydrogen pyrophosphate; ion exchange chromatography; lyophilization