One kind of n- [2- (2- hydroxyethoxy) -4-nitrophenyl] ethanolamine preparation

2015 
The present invention relates to an N-[2- (2- hydroxyethoxy) -4-nitrophenyl] ethanolamine production method, which is 2-amino-5-nitrophenol as starting material, 2-amino - 5-nitro-phenol mixture with a base and a solvent is added after hydroxyethylation agent, reacted to produce 2- (3-nitro-6-amino phenoxy) ethanol at a certain pressure and temperature; 2- (3-nitrophenyl -6-aminophenoxy) ethanol is then reacted with chlorine in the catalyst chloroformate, by condensation, hydrolysis to give N- [2- (2- hydroxyethoxy) -4-nitrophenyl] ethanolamine. The present invention has a high yield, high purity and good quality, gentle production process, produces less waste, etc; the present invention is not economic environment, and suitable for industrial production.
    • Correction
    • Source
    • Cite
    • Save
    • Machine Reading By IdeaReader
    0
    References
    0
    Citations
    NaN
    KQI
    []