Precursor Routes to Complex Ternary Intermetallics: Single‐Crystal and Microcrystalline Preparation of Clathrate‐I Na8Al8Si38 from NaSi + NaAlSi.

Yongkwan Dong,Ping Chai,Matt Beekman,Xiaoyu Zeng,Terry M. Tritt,George S. Nolas

Precursor Routes to Complex Ternary Intermetallics: Single‐Crystal and Microcrystalline Preparation of Clathrate‐I Na8Al8Si38 from NaSi + NaAlSi.

2015

Yongkwan Dong
Ping Chai
Matt Beekman
Xiaoyu Zeng
Terry M. Tritt
George S. Nolas

Microcrystalline clathrate-I compounds Na8AlxSi46-x (x = 4, 6, 8) are synthesized by spark plasma sintering using a NaSi/NaAlSi mixture as precursor (973 K, 3 h).

Keywords:

Spark plasma sintering
Intermetallic
Single crystal
Ternary operation
Chemical engineering
Microcrystalline
Inorganic chemistry
Clathrate hydrate
Chemistry

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