The burning issue of dung in archaeobotanical samples: a case-study integrating macro-botanical remains, dung spherulites, and phytoliths to assess sample origin and fuel use at Tell Zeidan, Syria

Since Naomi Miller’s first discussion of dung fuel within macro-botanical samples from Malyan, Iran, considerations of dung fuel across Southwest Asia have become commonplace, yet archaeobotanists remain divided on: (1) the extent to which dung fuel contributed to archaeobotanical assemblages relative to remnants of repeated crop processing and household activities; and (2) the plant-based, middle-range theories that should be used to infer the presence of dung within macro-botanical assemblages. Here we present a case-study integrating a simple, well-established geo-archaeological approach to assess the presence and relative abundance of dung spherulites within paired sediment and flotation samples from Ubaid period Tell Zeidan, Syria (5300–5100 bc). Spherulite data generated from “sediment smears” are integrated with macro-botanical and phytolith data to assess elevated concentrations of dung within samples. Our analyses demonstrate that plant-based depositional processes across a site are complex, reflecting the rich nature of plant use in antiquity. By using a multi-proxy approach, it is possible to differentiate between predominantly fuel-based deposits and those resulting from predominantly crop-processing processes with greater resolution. This study documents the use of wood fuels in hearths and dung fuel within pyrotechnic features and an oven during the Ubaid period, thereby contributing to discussions of fuel selection and the Secondary Products Revolution. When spherulites are preserved within sediment in abundance, they are also present in floated material, so it is possible to use this approach to consider the presence of dung within archived macro-botanical samples and resolve decade-old debates.