Sapphire optical viewport for high pressure and temperature applications
2021
We describe the design of a soldered sapphire optical viewport, useful for spectroscopic applications of samples at high temperatures and high pressures. The sapphire window is bonded via active soldering to a metal flange with a structure of two c-shaped rings made of different metallic materials in between, as to mitigate thermally induced stress. A spectroscopic cell equipped with two of the optical viewports has been successfully operated with alkali metals in a noble gas environment at temperatures in the range $20\,$°C to $450\,$°C at noble gas pressures from $10^{-6}\,$mbar to $330\,$bar. At the upper pressure range, we observe a leakage rate smaller than our readout accuracy of $30\,$mbar per day.
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