Chemiluminescence Determination of Tiopronin by Flow Injection Analysis Based on Cerium(IV) Oxidation Sensitized by Quinine
1997
A flow injection analysis method is proposed for the determination of
tiopronin based upon the oxidation by cerium(IV) in dilute
sulfuric acid medium and sensitized by quinine. With the peak height as a
quantitative parameter applying optimum working conditions, tiopronin is
determined over the 1–400 µM range (150 µl per
injection, n = 10, r = 0.9994) with a detection limit of
0.34 µM and an RSD (n = 10) less than 2% at 20 and
50 µM. The proposed method, combining the advantages of
speed and sensitivity, was applied to the routine determination of
tiopronin in a pharmaceutical preparation.
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