Synthesis of O-Nitrophenylacetaldehyde
2012
O-nitrotoluene is condensed with N, N-dimethylformamide dimethyl acetals in the presence of piperidine and DMF to yield trans-β-dimethylamino-2-nitrostyrene which undergoes hydrolysis in the 18% HCl aqueous solution to obtain o-nitrophenylacetaldehyde with yield of 83% and purity of 98.1% respectively.
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