SYNTHESIS AND CONFORMATION OF 2-SILYLETHYNYL-SUBSTITUTED 2,4,4,6-TETRAMETHYL-1,3-DIOXANES
1998
Reaction of 2,4,4,6-tetramethyl-1,3-dioxanium perchlorate with lotsich reagents led to the synthesis of new silylethynyl-substituted 2,4,4,6-tetramethyl-1,3-dioxanes. According to the data of1H and13C NMR and x-ray diffraction analysis, it was established that the 1,3-dioxane ring of the products obtained has the chair conformation.
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