Formic Acid-Driven Rapidand Green Anti-Markovnikov Hydrothiolation of Styrenes
2019
A novel formic acid-assisted rapid and efficient route for C–S bond construction via the thiol–ene reaction has been reported. Exclusively, the anti-Markovnikov product was obtained in good to excellent yield using the developed protocol. Various styrenes and thiols bearing different functionalities were well tolerated. The reaction also provided a good yield of sulfones in a one-pot two-step protocol. The developed method is operationally simple, green, metal-free, solvent-free, and having a high atom economy with high regioselectivity.
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