A highly selective method for 11β-OH protection of steroidal 11β, 17α-diols
2008
A highly selective method to protect the 11β-OH position of steroid (1) has been developed. This is achieved via double silyl protection of the 11β, 17α-diol, followed by selective desilylation of the 17α-OH under basic conditions without the need for a fluoride source.
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