Mass spectra of organosilicon peroxides
1986
1.
A method has been developed for mass-spectrometric examination of organosilicon peroxides, avoiding their easy decomposition and hydrolysis and enabling the obtention of their mass spectra for the first time.
2.
The peak of the Me3C+ ion has the highest intensity in the mass spectra of silyltert-butyl peroxides, while in the case of disilyl peroxide, it is the peak of the [Me2SiOSiMe2H]+ ion with a probable structure of a siloxane. The mass spectra obtained can be used for the analytical detection of peroxides and control of their purity.
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