Method for preparing graphene-epoxy resin composite material

2010 
The invention provides a method for preparing a graphene-epoxy resin composite material, comprising the following steps of mixing epoxy resin and a graphene solution in ratio; controlling the temperature at 60-120 DEG C; stirring for 5-60min; standing for 30min to layer; pouring out an aqueous solution at the upper layer; continuously stirring graphene-epoxy resin at the lower layer at the temperature of 80-150 DEG C and reactng for 2-12h; adding an epoxy resin curing agent, curing for 1h at the temperature of 100 DEG C, and then curing for 2h at the temperature of 150 DEG C, wherein the used epoxy resin is bifunctional bisphenol A epoxy resin or bifunctional epoxy resin. The method has the advantages of no environmental pollution in aqueous-phase reaction, recyclable water at the upper layer, simple operation process and controllable loading and is easy for preparation and synthesis in large scale. The prepared graphene-epoxy resin composite material has good monodispersity. Compared with an epoxy resin composite material, the rigidity of the prepared graphene-epoxy resin composite material is increased by above 50 percent, and the impact resistance is increased by near 12 times.
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