Synthesis of β-BaB2O4 thin films from a metallorganic precursor
1997
β-BaB
2
O
4
(β-BBO) thin
films have been successfully synthesized by the sol–gel method from
a BBO precursor solution. A stable BBO precursor solution was prepared
from barium metal and boron triethoxide in a mixed solvent of ethanol and
2-ethoxyethanol. The precursor films crystallized into β-BBO
on glass (Corning 7059) and fused silica substrates at 550 °C. BBO
films on glass (Corning 7059) and fused silica substrates showed a highly
(006) preferred orientation. The absorption edge of β-BBO
films on fused silica substrates was at <190 nm. The
β-BBO films on glass (7059) and fused silica substrates
showed second harmonic generation (SHG) of 532 nm light upon irradiation
with 1064 nm Nd:YAG laser light. The SH power from the BBO films has been
correlated with the fundamental power through the square-law
proportionality based on theory.
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