Device and method for testing electric conductivity of powder material and impedance of membrane electrode
2013
The invention provides a device and a method for testing the electric conductivity of a powder material and the impedance of a membrane electrode, which can meet two measurement modes: a powder material electric conductivity measurement mode and a membrane electrode impedance measurement mode. The powder material electric conductivity measurement mode comprises the steps of putting a testing sample of prepared powder press cake in a sample testing cell, testing by using an assembled die, obtaining the total impedance and electron impedance of powder respectively, obtaining proton impedance by combining an impedance parallel-connection formula and calculating to obtain electron conductivity, proton conductivity and total conductivity; and the membrane electrode impedance measurement mode comprises the steps of putting a testing sample of the prepared membrane electrode in the sample testing cell, testing by using the assembled die and obtaining the impedance of a membrane electrode. The testing device is provided with a temperature control sleeve and a humidifying pipeline, so that the electric conductivity of the powder material and the impedance of the membrane electrode under different temperature and humidity can be tested. The testing device is simple in equipment, easy to operate and precise in measurement result; meanwhile, the testing device is applicable for testing the electric conductivity of a mixed charged powder material and the impedance of the membrane electrode in a simulative PEM (Polymer Electrolyte Membrane) electrolytic tank environment; and therefore, the feasibility, the necessity and the importance of the device are further highlighted.
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