Synthesis and flash vacuum pyrolysis of isoxazolo- and isothiazolo[5,4-d]pyrimidines
1994
The multi-step synthesis of isothiazolo[5,4-d]pyrimidines (1c,d) and isoxazolo[5,4-d]pyrimidine (1b) is described. Flash vacuum pyrolysis of lb leads to phenyliminopropadienone, Ph-N=C=C=C=O, which was identified by Ar matrix infrared spectroscopy.
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