Synthesis of Fe3O4 nanoparticles and formation of nanowire by electrophoretic deposition
2007
Abstract Template-growth of Fe 3 O 4 nanowires via electrophoretic deposition (EPD) was investigated. The solution for EPD was aqueous solution with uniformed dispersed Fe 3 O 4 nanoparticles. Black-colored and single spinel phase of Fe 3 O 4 nanoparticles were easily obtained by hydrothermal method using ferric chloride and ferrous chloride as starting materials. Single spinel phase only form when all precursors were dissolved in a basic solution ( pH > 9 ) . Ratio of iron (II) to iron (III) is important for the formation of Fe 3 O 4 single spinel phase. The diameter of Fe 3 O 4 nanoparticles obtained is around 20–30 nm. Fe 3 O 4 nanowires with length more than 20 μ m and diameter around 130–150 nm are successfully synthesized. Scanning electron microscopy (SEM) image, transmission electron microscope (TEM), powder X-ray diffraction (XRD) and vibrating sample magnetometer (VSM) were employed to characterize the products.
Keywords:
- Ferric
- Scanning electron microscope
- Nanoparticle
- Nanowire
- Ferrous
- Physics
- Nanotechnology
- Nuclear magnetic resonance
- Chloride
- Electrophoretic deposition
- Inorganic chemistry
- Electron microscope
- Transmission electron microscopy
- Hydrothermal synthesis
- Chemical engineering
- Spinel
- Aqueous solution
- Condensed matter physics
- Correction
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