Effect of grain size on the low-cycle fatigue behavior of carbon-containing high-entropy alloys

Abstract The effect of grain size on tensile and cyclic deformation behaviors of carbon-containing CoCrFeMnNi high-entropy alloys (Cantor) were investigated. Heat treatment of warm-rolled and cold-rolled specimens yielded various microstructures with average grain sizes 4 ≤ d ≤ 66 μm. The fine-grained specimens (d ≤ 15 μm) showed very similar tensile deformation behaviors. However, in the coarse-grained specimen (d ∼ 66 μm) formation of mechanical twins led to different strain-hardening behavior than in the fine-grained ones. Refining d to 10 μm by decreasing the heat-treatment temperature after warm rolling increased the strength and extended low-cycle fatigue life. However, no significant change in fatigue cycles occurred in that they could survive at similar imposed plastic strain amplitudes. The smallest d ∼4 μm with the best yield strength was achieved after heat-treating the cold-rolled specimens at 800 °C; the grain size decrease was accompanied by formation of coarse carbides. High stress concentrations developed at the boundaries of these coarse particles with the matrix, and severely reduced fatigue life. Thus, to increase the fatigue life in carbon-containing Cantor, thermomechanical treatment should be controlled in such a way that results in fine-grained microstructures without precipitation of coarse carbides.