Impurity analysis of Tamoxifen and Toremifene samples obtained by McMurry reaction

2005 
The structure of two impurities of commercial samples of tamoxifen (CAS 10540-29-1) and toremifene (CAS 89778-26-7), prepared by McMurry procedure, were characterised by spectroscopic methods. The two impurities were found to be strictly connected with the synthesis procedure. Their detection can be useful to trace back the synthesis route of a sample.
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