Two-photon-excited, three-dimensional photoluminescence imaging and dislocation-line analysis of threading dislocations in 4H-SiC

This paper describes the three-dimensional imaging of threading edge dislocations ( TEDs), pure c threading screw dislocations ( TSDs), and c + a threading mixed dislocations ( TMDs) in 4H silicon carbide (4H-SiC) epilayers by two-photon-excited photoluminescence (2PPL), where inclinations of dislocations in epilayers with different offcut angles are investigated. A numerical model based on carrier diffusion explains the mechanism of the dark-contrast 2PPL imaging provided by band edge emission. More than 450 threading dislocations in 4H-SiC epilayers are visualized three-dimensionally and are classified into six -type TEDs, two -type TSDs, and twelve -type TMDs according to the directions of extra half-planes and the chiral geometries (right- or left-handed screw). The 2PPL images reveal that all threading dislocation types incline in the step-flow direction, the extent of which is more prominent for a larger offcut angle. The TEDs also incline in the directions of their extra h...