Bi2SiO5 nanosheets prepared by molten salt method

2012 
Bi2SiO5 nanosheets were successfully synthesized by the molten salt method in NaCl–Na2SO4 flux using Bi2O3 and SiO2 as raw materials. XRD analysis and SEM observation show that the incorporation of salt medium can greatly lower the formation temperature of Bi2SiO5 phase, and promote their crystallization. The results also demonstrate that the mass ratio of salts to reactants, the reaction time, and the calcination temperature have significant effects on the phase formation and morphology of the Bi2SiO5 powders. The UV–vis spectra result shows that the absorption of the Bi2SiO5 powders located at 380 nm, and the corresponding band gap energy (Eg) calculated is 3.26 eV.
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