The fatigue crack propagation tests for circular notched compact tension specimens of GH4133B superalloy used in a turbine disk of aero-engine are carried out at room temperature. The test data shows that in the transition region from short to long crack growth, the crack growth rate appears as a fluctuation form with acceleration following deceleration. A quasi harmonic function is constructed to model the fatigue crack growth in the transition region, and the result indicates that such function is suitable to describe the crack growth behavior. A metallographic analysis with respect to microscopic observation for the specimen’s surface suggests that the wave period, that is, a step length of a cycle fluctuation from acceleration to deceleration on the crack growth rate curve is agree well with the intrinsic scale of grain size, which indicates that in the transition region from short to long crack growth, grain boundary plays a dominant role in crack growth rate. Finally, the fracture surfaces of specimen are observed using a scanning electron microscopy. It can be found from the fracture surface morphologies that in the transition region from short to long crack growth, the stress intensity factor range is still lower than the fatigue crack growth threshold Δ K th , the effect of microstructure, such as grain size, grain boundary, secondary phase particle, and inclusion ahead of the crack tip, and the effect of crack closure on crack growth behavior should be considered, the local further plastic deformation at crack tip will meet larger resistance, so some twin bands are observed on the fracture surface. As crack length increases with increasing fatigue cycle, the crack propagation is noted to change from a transgranular crack propagation mode, a mixed transgranular and intergranular crack propagation nature, to intergranular crack propagation manner.
The high cycle fatigue tests for smooth specimens of TC25 titanium alloy under different stress ratios are carried out on a MTS 809 Material Test Machine at a given maximum stress level of 917MPa at ambient temperature, the high cycle fatigue lifetimes for such alloy are measured, and the effects of stress amplitude and mean stress on high cycle fatigue life are analyzed. The initial resistance is measured at the two ends of smooth specimen of TC25 titanium alloy, every a certain cycles, the fatigue test is interrupted, and the current resistance values at various fatigue cycles are measured. The ratio of resistance change is adopted to characterize the fatigue damage evolution in TC25 titanium alloy, and a modified Chaboche damage model is applied to derive the fatigue damage evolution equation. The results show that the theoretical calculated values agree well with the test data, which indicates that the modified Chaboche damage model can precisely describe the accumulated damage in TC25 titanium alloy at high cycle fatigue under unaxial loading. Finally, the high cycle fatigue lifetimes for TC25 titanium alloy specimens at different strain hardening rates are tested at a given stress ratio of 0.1, the effect of strain hardening on fatigue life is investigated based on a microstructure analysis on TC25 titanium alloy, and an expression between fatigue life and strain hardening rate is derived
The catalytic activity was enhanced by the introduction of C18PA on the support of the Ru/Nb 2 O 5 catalyst. The addition of more Lewis acid sites on the support activated the aromatic ring in phenol and promoted the formation of cyclohexanol.
The short fatigue crack growth tests for circular notched compact tension specimens of GH4133B superalloy used in turbine disk of aero-engine are carried out at ambient temperature and atmospheric pressure. The stress intensity factor ranges and the fatigue crack growth rates at various stress ratios are measured, and the corresponding effective stress intensity factor ranges considering the crack closure effect are calculated. It is shown that the effective stress intensity factor range Δ K eff , can be applied to describe the deceleration and acceleration of crack growth rate during the short crack propagation. The fatigue fracture surface morphologies in the short crack growth region are investigated using a scanning electron microscopy. It is found that there is a cleavage step between two adjacent radial striations, a series of early fatigue striations exist on the cleavage step, and some secondary cracks perpendicular to the direction of main crack propagation emerge on the fracture surface, the superalloy exhibits a mixed fracture mode in the short crack growth region, which reveals the microscopic mechanism of short crack propagation that the fatigue crack growth rate is primarily higher, and then gradually decreases with the propagation of short crack.
Acid fracturing, with a pumping pressure up to 140 MPa for fractural liquid injection, is commonly used in enhanced oil recovery. Subjected to severely high hoop stress, stress corrosion cracking (SCC) often occurs at cracks inside manifold elbows which are due to acid corrosion and fracturing propping agent erosion. To avoid the occurrence of SCC, it is necessary to establish a substantial understanding of the fracture strength of thick-walled elbow, including the stress state distribution in elbow and SCC properties of elbow material. Base on the hoop stress calculation for thin wall straight pipe, a formula for hoop stress of thick-walled elbow is derived and also verified with finite element method (FEM). This is accomplished by introduce curvature factor and wall thickness factor into the formula. Furthermore, the critical stress intensity factor, KISCC, is determined subsequently in simulated acid fracturing corrosion condition. However, part of the considerable contribution of this work is to scale the critical crack depth. A simplified hoop stress formula proposed in this paper can be used in design of elbow wall thickness and strength evaluation. The established critical crack depth calculation formula can be applied to safety assessment of elbows with initial erosion cracks. The proposed method has been proved to be a simple and useful method to calculate the stress and fractural strength of thick-walled elbow.
The fatigue crack growth tests for nickel-based GH4133B superalloy used in turbine disk of a type of aero-engine are carried out at room temperature. The stress intensity factor ranges and the fatigue crack growth rates at various stress ratios are measured, and the corresponding threshold stress intensity factor ranges are determined. Using the Paris formula, the experiment data of fatigue crack growth are analyzed. It is shown that the fatigue crack growth rate increasing with increasing stress intensity factor range and stress ratio, and a modified Paris formula considering threshold stress intensity factor range can describe the fatigue crack growth behavior precisely. The fracture surface morphologies are investigated using a scanning electron microscope. It is shown that in the crack initiation region, steady growth region and rapid growth region, the fracture surface exhibits a cleavage fracture mode, fatigue striations and an intergranular fracture mode, respectively. Finally, the von Mises stresses and stress intensity factors at the crack tip of specimen of GH4133B superalloy at various external loads and crack lengths are simulated using the finite element method, and the threshold stress intensity factors under different maximal external loads at a certain crack length are calculated. The comparison between test and simulation indicates that the stress intensity factors at the crack tip calculated by the finite element method agree well with experimental data.