Arnold W. By

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ChemInform Abstract: TOTAL SYNTHESIS OF STEROIDAL DERIVATIVES PART 4, SYNTHETIC STUDIES IN THE VERATRUM ALKALOID SERIES PART 1, INTRODUCTION AND THE TOTAL SYNTHESIS OF APPROPRIATE C-NOR-D-HOMO STEROID DERIVATIVES

Chemischer Informationsdienst (1975)

James P. Kutney Arnold W. By John Cable W. A. F. Gladstone T. Inaba

10.1002/chin.197539379

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Citations (0)

A Direct Synthesis of O⁶-Monoacetylmorphine from Morphine

Canadian Society of Forensic Science Journal (1985)

Wing-Wah Sy Arnold W. By George A. Neville William L. Wilson

O6-Monoacetylmorphine was synthesized directly in good yield from morphine with glacial acetic acid using sulphuric acid as a catalyst. The product was characterized by PMR, IR, MS, and elemental microanalysis. This successful synthesis of O6-monoacetylmorphine from morphine shows that this compound can be included under the Narcotic Control Act as a regulated substance for legal purposes.

Microanalysis

10.1080/00085030.1985.10757388

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Citations (8)

TOTAL SYNTHESIS OF STEROIDAL DERIVATIVES: II. SYNTHESIS OF HYDROCHRYSENE ANALOGUES AND RELATED COMPOUNDS

Canadian Journal of Chemistry (1963)

James P. Kutney J H Winter Wm. McCrae Arnold W. By

A synthetic sequence leading to the total synthesis of hydrochrysene derivatives possessing the trans–anti–trans backbone is described. The introduction of a ketonic function into ring C of these compounds is also given. It is noted that these substances allow entry into the synthesis of intermediates which have an open ring C.

Sequence (biology)

10.1139/v63-065

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Citations (6)

Steroid hormone analogs. IV. C-Nor-D-homoestrone

The Journal of Organic Chemistry (1968)

S. Morris Kupchan Arnold W. By Michael S. Flom

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTSteroid hormone analogs. IV. C-Nor-D-homoestroneS. Morris Kupchan, Arnold W. By, and Michael S. FlomCite this: J. Org. Chem. 1968, 33, 2, 911–914Publication Date (Print):February 1, 1968Publication History Published online1 May 2002Published inissue 1 February 1968https://pubs.acs.org/doi/10.1021/jo01266a117https://doi.org/10.1021/jo01266a117research-articleACS PublicationsRequest reuse permissionsArticle Views41Altmetric-Citations8LEARN ABOUT THESE METRICSArticle Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. These metrics are regularly updated to reflect usage leading up to the last few days.Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Find more information about Crossref citation counts.The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Find more information on the Altmetric Attention Score and how the score is calculated. Share Add toView InAdd Full Text with ReferenceAdd Description ExportRISCitationCitation and abstractCitation and referencesMore Options Share onFacebookTwitterWechatLinked InRedditEmail Other access optionsGet e-Alertsclose Get e-Alerts

Steroid hormone

10.1021/jo01266a117

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Citations (8)

¹³C NMR of some aryl‐methylated trans‐β‐methyl‐β‐nitrostyrenes

Magnetic Resonance in Chemistry (1993)

Brian A. Dawson Arnold W. By Hajro W. Avdovich

Abstract The 13 C NMR chemical shifts of ten arylmethylated trans ‐β‐methyl‐β‐nitrostyrenes and the parent compound were measured and the spectra interpreted. Chemical shift assignments for the aryl‐methylated compounds have not, to our knowledge, been reported previously. The data are based on 1 D and 2D experiments performed at 9.4 T.

Chemical shift

Cis–trans isomerism

Proton NMR

10.1002/mrc.1260310121

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Citations (2)

Identification of the iV-Methylated Analogs of the Hallucinogenic Amphetamines and Some Isomers

Journal of AOAC INTERNATIONAL (1975)

Keith Bailey Arnold W. By Donald Legault Denise Verner

The drugs 2-, 3-, and 4-methoxy-N-methylamphetamine, 3-methoxy-4,5-methylenedioxy-N-methylamphetamine, and 3,4-methylenedioxy-N-methylamphetamine are identified by spectroscopic techniques. The ultraviolet and mass spectra of isomers are similar, but proton magnetic resonance and infrared spectra are distinctly different, and reference spectra and data are provided. Gas-liquid and thin layer chromatographic systems for the analysis are discussed.

Identification

Designer drug

10.1093/jaoac/58.1.62

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Citations (17)

Syntheses of 3-O- and 6-O-Propanoylmorphine—A Reinvestigation and Correction

Journal of Pharmaceutical Sciences (1986)

Wing-Wah Sy Arnold W. By George A. Neville William L. Wilson

10.1002/jps.2600750813

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Citations (7)

Nitration of substituted styrenes with nitryl iodide

Tetrahedron Letters (1985)

Wing-Wah Sy Arnold W. By

Triethylamine

10.1016/s0040-4039(00)98431-4

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Citations (45)

A totally synthetic entry into the veratrum alkaloid skeleton

Tetrahedron Letters (1965)

James P. Kutney Arnold W. By T. Inaba Sim Y. Leong

Skeleton (computer programming)

10.1016/s0040-4039(00)90236-3

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Citations (9)

CHEMICAL AND PHYSICAL PROPERTIES OF (Z)—AND (E) -MONOETHOXY-1-(2-NITRO-1-PROPENYL) BENZENES: Important Precursors to the monoethoxyamphetamines

Canadian Society of Forensic Science Journal (1990)

Arnold W. By Bruce A. Lodge Wing-Wah Sy J. Zámečník Randy M. Duhaime

(Z)-Monoethoxy-1- (2-nitro-1-propenyl)benzenes were synthesized from the corresponding (E)-isomers by irradiation with light in toluene in the presence of benzophenone. The gas-liquid chromatographic (GLC) and thin-layer chromatographic (TLC) data, and ultraviolet (UV), infrared (IR), proton magnetic resonance (1H-NMR), and mass spectra (MS) are presented for both isomers for comparison. The (Z)-isomer is partially converted on the injector of GLC apparatus to the (E)-isomer.

Propenyl

Ultraviolet

Proton NMR

Cis–trans isomerism

10.1080/00085030.1990.10757454

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Citations (5)