Azadeh Jani

Imam Khomeini International University

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Shima Nasri

Imam Khomeini International University

Mohammad Bayat

Imam Khomeini International University

Rahman Alivisi

Islamic Azad University, Science and Research Branch

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Imam Khomeini International University

Tehran University of Medical Sciences

Amirkabir University of Technology

Arak University of Medical Sciences

University of Tehran

Tarbiat Modares University

Islamic Azad University, Ashtian Branch

Bu-Ali Sina University

Ilam University

Islamic Azad University, Science and Research Branch

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Novel synthesis of oxoacetamides via reaction of salicylaldehyde and isocyanide under mild reaction condition

Heliyon (2020)

Mohammad Bayat Shima Nasri Rahman Alivisi Azadeh Jani

A convenient procedure for the formation of oxoacetamides derivatives is reported via the reaction of salicylaldehyde and alkyl isocyanide in a simple process without the use of any catalyst or metal promoters in DCM at room temperature. The structure of all obtained derivatives were determined by elemental and spectral analyses. In this reaction, 1,3-dioxine-4,4-dicarboxamide was obtained as minor product. This process offers considerable advantages such as the simplicity of reaction, regioselectivity, and the use of commercially available materials.

Salicylaldehyde

Reaction conditions

10.1016/j.heliyon.2020.e04076

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