Qiao‐Lin Wang

Hunan Institute of Science and Technology

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Quan Zhou

Taizhou University

Kewen Tang

Hunan Institute of Science and Technology

Biquan Xiong

Hunan Institute of Science and Technology

Yun Liang

Hunan Normal University

Pu Chen

Baoji University of Arts and Sciences

Yu Liu

Hunan Institute of Science and Technology

Yu Liu

Hunan Institute of Science and Technology

Congshan Zhou

Hunan Institute of Science and Technology

Zan Chen

China National Offshore Oil Corporation (China)

Panliang Zhang

Hunan Institute of Science and Technology

Cooperative Institutions

Hunan Institute of Science and Technology

Peking University

Xiangtan University

Hunan Normal University

Wuhan University of Technology

South China University of Technology

Sinopec (China)

Capital Medical University

Central South University

Inner Mongolia Electric Power (China)

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Iron‐Mediated Cyanoalkylsulfonylation/Arylation of Active Alkenes with Cycloketone Oxime Derivatives via Sulfur Dioxide Insertion

Advanced Synthesis & Catalysis (2020)

Zan Chen Quan Zhou Qiao‐Lin Wang Pu Chen Biquan Xiong

Abstract Iron‐mediated radical cyanoalkylsulfonylation/arylation of active olefins with cycloketone oxime derivatives via cleavage of C−C single bond and insertion of SO 2 is developed for the preparation of cyanoalkylsulfonylated oxindoles. This difunctionalization of carbon−carbon double bond via a radical pathway involves cyclobutanone oxime ester fragmentation, sulfonyl radical generation and radical addition/5‐ exo cyclization. The methodology displays good functional group tolerance and does not require any external bases or oxidants. magnified image

Sulfonyl

Functional group

Cyclobutanone

Radical cyclization

10.1002/adsc.202000369

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Citations (47)

Transition Metal‐Free Difunctionalization of C−C Bond with Sodium Sulfinates and Water Leading to (E)‐1‐Phenyl‐4‐sulfonylbut‐1‐enes

Advanced Synthesis & Catalysis (2019)

Qiao‐Lin Wang Zan Chen Quan Zhou Congshan Zhou Biquan Xiong

Abstract Without using any transitionmetal and base, an eco‐friendly, practical and economical protocol has been established for the one‐pot synthesis of diverse ( E )‐1‐phenyl‐4‐sulfonylbut‐1‐enes from easily accessible starting materials. This strategy features a wide substrate scope, tolerates a broad range of functional groups, employs a less expensive oxidant, is operationally simple, and can be easily scaled‐up. magnified image

Scope (computer science)

Base (topology)

10.1002/adsc.201801475

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Citations (10)