Bill Morandi

Abstract The new approach includes diazotation of trifluoroethylamine (I) followed by ZrCl 4 ‐promoted reaction of the resulting trifluorodiazoethane with aldehydes.

10.1002/chin.201208072

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CCDC 2256057: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Patrick Müller Patrick Finkelstein Nils Trapp Alessandro Bismuto Gunnar Jeschke

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2fqm1v

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Iron-Catalyzed Cyclopropanation with Glycine Ethyl Ester Hydrochloride in Water

Organic Letters (2012)

Bill Morandi Amund Dolva Erick M. Carreira

An iron-catalyzed cyclopropanation reaction of styrenes in aqueous media is disclosed that employs glycine ethyl ester hydrochloride in a tandem diazotization/cyclopropanation reaction. The products are accessed in good yields and good diastereoselectivity using readily available and inexpensive starting materials. Moreover, a wide range of transition metals may be used under these conditions, thus opening new opportunities for efficient carbene-transfer reactions under user-friendly conditions.

Hydrochloride

Tandem

10.1021/ol300688p

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CCDC 2256061: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Patrick Müller Patrick Finkelstein Nils Trapp Alessandro Bismuto Gunnar Jeschke

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2fqm5z

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CCDC 2157542: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Xichang Dong Martin Klein Siegfried R. Waldvogel Bill Morandi

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2bf341

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CCDC 2217024: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Michael K. Bogdos Patrick Müller Bill Morandi

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2ddzxq

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CCDC 2157547: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Xichang Dong Martin Klein Siegfried R. Waldvogel Bill Morandi

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2bf396

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CCDC 2266361: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Yannick Brägger Ori Green Benjamin N. Bhawal Bill Morandi

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2g2bfb

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CCDC 2256066: Experimental Crystal Structure Determination

The Cambridge Structural Database (2023)

Patrick Müller Patrick Finkelstein Nils Trapp Alessandro Bismuto Gunnar Jeschke

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccdc.csd.cc2fqmb4

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Nitrogen atom insertion into indenes to access isoquinolines

Patrick Finkelstein Julia C. Reisenbauer Ori Green Bence B. Botlik Andri Florin

We report a convenient protocol for a nitrogen atom insertion into indenes to afford isoquinolines. The reaction uses a combination of commercially available (diacetoxy¬iodo)benzene (PIDA) and ammonium carbamate to furnish a wide range of isoquinolines. Various substitution patterns and commonly used functional groups are well tolerated and the operational simplicity renders this protocol broadly applicable. Furthermore, this strategy enables the facile synthesis of 15N labeled isoquinolines, using 15NH4Cl as a commercial 15N source.

Carbamate

Nitrogen atom

Isoquinoline

10.26434/chemrxiv-2022-cgcdk

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