Xianxian Duan

Huazhong University of Science and Technology

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Zengwei Luo

Huazhong University of Science and Technology

Yuling Lu

Huazhong University of Science and Technology

Hucheng Zhu

Huazhong University of Science and Technology

Chunmei Chen

Huazhong University of Science and Technology

Yonghui Zhang

Huazhong University of Science and Technology

Lianghu Gu

Huazhong University of Science and Technology

Meng Yao

Changzhou University

Xia Chen

Wuhan University of Science and Technology

Zhenhua Guan

Huazhong University of Science and Technology

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Huazhong University of Science and Technology

Chinese Academy of Sciences

Changzhou University

University of Chinese Academy of Sciences

Southern University of Science and Technology

Wuhan University of Science and Technology

Tongji Hospital

Wuhan University

Hubei University

Shandong University of Technology

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A mild tetradehydro-Diels–Alder reaction of aryldiyne compounds affords exclusively linear products

Organic & Biomolecular Chemistry (2022)

Yuling Lu Xianxian Duan Xia Chen Meng Yao Chunmei Chen

A mild aromatic tetradehydro-Diels–Alder reaction of aryldiynes is described for linear substituted naphthalenes.

Diels–Alder reaction

Reaction conditions

10.1039/d2ob00121g

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A Removable Acyl Group Promoted the Intramolecular Dehydro-Diels–Alder Reaction of Styrene-Ynes: Highly Chemoselective Synthesis of Aryldihydronaphthalene Derivatives

The Journal of Organic Chemistry (2022)

Xia Chen Cheng Zhong Xianxian Duan Zhenhua Guan Lianghu Gu

A removable acyl group promoted the intramolecular didehydro-Diels–Alder reaction of styrene-ynes under mild reaction conditions is proposed. The reaction is free of metals and catalysts, is easy to perform, and exhibits good functional group tolerance, providing a highly chemoselective approach for obtaining the valuable aryldihydronaphthalene derivatives.

Diels–Alder reaction

Functional group

10.1021/acs.joc.2c00180

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Citations (7)

K₂S₂O₈-Mediated Radical Cyclization of 1,6-Enyne for the Synthesis of Diiodonated γ-Lactams

The Journal of Organic Chemistry (2023)

Yuling Lu Jiale Zhang Xianxian Duan Boyi Yang Chunhua Zhao

A novel and convenient K2S2O8-mediated diiodo cyclization of 1,6-enynes for the facile synthesis of functionalized γ-lactam derivatives has been developed. This reaction features mild and transition-metal-free conditions, which offer a green and efficient entry to synthetically important γ-lactam scaffolds. Mechanistic studies suggest that iodide radicals initiate the cascade cyclic transformation.

Enyne

Lactam

Radical cyclization

10.1021/acs.joc.2c02818

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CCDC 2117835: Experimental Crystal Structure Determination

The Cambridge Structural Database (2022)

Yuling Lu Xianxian Duan Xia Chen Meng Yao Chunmei Chen

10.5517/ccdc.csd.cc292s8g

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