In this Dataset it is possible to observe the effect of the lateral needles, or stigmators, of the Sorter1 on a slightly out of focus probe. The theory behind this device can be found at 10.1016/j.ultramic.2019.112861
It has recently been shown that an electron vortex beam can be generated by the magnetic field surrounding the tip of a dipole-like magnet. This approach can be described using the magnetic Aharonov-Bohm effect and is associated with the fact that the end of a long magnetic rod can be treated approximately as a magnetic monopole. However, it is difficult to vary the magnetisation of the rod in such a setup and the electron beam vorticity is fixed for a given tip shape. Here, we show how a similar behaviour, which has the advantage of easy tuneability, can be achieved by making use of the electrostatic Aharonov-Bohm effect associated with an electrostatic dipole line. We highlight the analogies between the magnetic and electrostatic cases and use simulations of in-focus, Fresnel and Fraunhofer images to show that a device based on two parallel, oppositely charged lines that each have a constant charge density can be used to generate a tuneable electron vortex beam. We assess the effect of using a dipole line that has a finite length and show that if the charge densities on the two lines are different then an additional biprism-like effect is superimposed on the electron-optical phase.
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A novel nanostructured cemented carbide formed from WC-5%Co-20%BNi2 brazing alloy is described. During sintering, the BNi2 alloy is infiltrated into a green compact of WC-5%Co at 1050-1100 {\deg}C for 2-60 minutes. Perfect wetting behavior and a zero contact angle are achieved after only 40 s. Relative densities of 98.5% and 100% and microhardness values of above 1500HV1 and 1800HV1 are obtained after 2 and 30 minutes, respectively. A change in mean particle size of about 600 nm in the precursor to a bimodal distribution of 350-400 nm and 10-20 nm is explained by a solution/reprecipitation mechanism.
In 1949, at the end of a paper dedicated to the concept of the refractive index in electron optics, Ehrenberg and Siday noted that wave-optical effects will arise from an isolated magnetic field even when the rays themselves travel in magnetic-field-free space. They proposed a two-slit experiment, in which a magnetic flux is enclosed between interfering electron beams. Now, through access to modern nanotechnology tools, we used a focused ion beam to open two nanosized slits in a gold-coated silicon nitride membrane and focused electron beam induced deposition to fabricate a thin magnetic bar between the two slits. We then performed Fraunhofer experiments in a transmission electron microscope equipped with a field emission gun and a Lorentz lens. By tilting the specimen in the objective lens field of the electron microscope, the magnetization of the bar could be reversed and the corresponding change in the phase of the electron wave observed directly in the form of a shift in the interference fringe pattern.
Franhofer diffraction dataset of electron vortex beams (EVBs) generated by the chopstic/MINEON device observed with a Camera Length of 205m on the K2 camera of the Titan Holo present in the Ernst-Ruska Centre at FZ-Julich. In this dataset, which can be accessed through Digital Micrograph and STEM_Cell it is possible to observe how by changing the potential difference between the two tips (main electrodes of the device) the radius of the EVB increases. A striking feature is that the radius increases almost linearly with the Orbital Angular Momentum. The analisys of this dataset can be found.at https://arxiv.org/abs/2203.00477
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