Jia-Zhuo Li

Nanjing Tech University

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De‐Cai Wang

Nanjing Tech University

Bo-Rong Leng

Nanjing Tech University

Yi‐Long Zhu

Nanjing Tech University

Qingquan Liu

Hunan University of Science and Technology

Yu-Lin Zhai

Soochow University

Yu‐Wen Huang

Nanjing Tech University

Yanjing Wang

Hunan University

Xin-Chao Meng

Nanjing Tech University

Luan-Ying Li

Nanjing Tech University

Xiyu Zhang

Tsinghua University

Cooperative Institutions

Nanjing Tech University

Chinese University of Hong Kong

Huazhong University of Science and Technology

Jiangsu Normal University

Nanjing Polytechnic Institute

Peking University

Harbin Institute of Technology

Shandong University of Science and Technology

Hunan University

Chinese Academy of Sciences

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Palladium-catalyzed regioselective hydrosulfonylation of allenes with sulfinic acids

RSC Advances (2022)

Luan-Ying Li Bo-Rong Leng Jia-Zhuo Li Qingquan Liu Jian‐Guang Yu

A simple palladium-based catalytic system for hydrosulfonylation of allenamides was established. Various nitrogen-containing linear allylic sulfones can be generated in moderate to excellent yield with E -selectivity and 100% atom utilization.

Sulfinic acid

Sulfone

Nitrogen atom

10.1039/d1ra09036d

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Photocatalytic selective synthesis of (E)-β-aminovinyl sulfones and (E)-β-amidovinyl sulfones using Ru(bpy)₃Cl₂ as the catalyst

RSC Advances (2024)

Yu‐Wen Huang Jia-Zhuo Li Feng Yang Xiyu Zhang Yanjing Wang

A photocatalytic strategy has been developed for the selective synthesis of ( E )-β-aminovinyl sulfones and ( E )-β-amidovinyl sulfones through the utilization of allenamides and sodium sulfinates.

10.1039/d3ra08272e

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Citations (1)

CCDC 2145528: Experimental Crystal Structure Determination

The Cambridge Structural Database (2022)

Yu-Lin Zhai Hui Zhou Qingquan Liu Bo-Rong Leng Zixian Zhang

10.5517/ccdc.csd.cc2b0llk

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Photocatalytic Markovnikov-type addition and cyclization of terminal alkynes leading to 4-sulfonyl quinoline-2(1H)-ones

Chemical Communications (2022)

Yu-Lin Zhai Hui Zhou Qingquan Liu Bo-Rong Leng Zixian Zhang

A new and expedient photocatalytic protocol for the construction of quinolin-2(1H)-ones via Markovnikov-type sulfonylation/6-endo-trig cyclization/selective C(O)-CF3 bond cleavage starting from N-alkyl-N-(2-ethynylphenyl)-2,2,2-trifluoroacetamides and sulfinic acids has been developed. It is as an unprecedented protocol for the preparation of 4-sulfonylquinoline-2(1H)-ones with high efficiency, mild reaction conditions, acceptable yields and a wide range of substrates.

Markovnikov's rule

Sulfonyl

Sulfinic acid

Quinoline

10.1039/d2cc01169g

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Photocatalytic Radical Cascade Dehalogenation/Carbo-cyclization/Sulfonylation Leading to Indole- and Benzofuran-Based Benzylic Sulfones

The Journal of Organic Chemistry (2023)

Qingquan Liu Jia-Zhuo Li Yanjing Wang Yan-Ning Leng Yu‐Wen Huang

This study presents a convenient approach to the synthesis of indole- and benzofuran-based benzylic sulfones using unactivated alkynes containing aryl iodides and sodium sulfinates under visible light irradiation. The procedure involves a sequential series of dehalogenation, carbo-cyclization, and radical sulfonylation. Plausible insights into the reaction mechanism are derived from control experiments, leading to the proposal of a radical cascade reaction pathway.

Benzofuran

Cascade reaction

10.1021/acs.joc.3c02068

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Citations (3)